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Wednesday, January 8, 2020

DIY Scanning Electron Microscope - Sources, Costs and References--- make money online

DIY Scanning Electron Microscope - Sources, Costs and References--- make money online

hey guys first off I want to give a big
thanks for all the subscriptions and
comments and views the project has
generated much more interest than I

would have imagined so it's really cool
to see people interested in this kind of
stuff second I saw a lot of comments
about back to the future in DeLorean so
I thought we'd take a little trip out to
the driveway Great Scott
this is my 1982 DeLorean which I've
owned for the past twelve years about
and I don't drive it every day I have a
Civic for that and I take this to car
shows about two or three shows a year so
this year I will be at West Coast dream
machines in Half Moon Bay and on a May
first alright well I hope you enjoyed
that now let's get down to business what
do you need to make a electron
microscope and how much is it going to
cost alright let's get started so here
is a really rough schematic of the
microscope I'm sorry for my poor drawing
ability but this is basically the
electron column over here so this is the
filament at the top the electron gun the
electrons proceeded down the column this
is where your sample would be and this
is the secondary detector so my goal
here is just to give you an idea of what
the main components are what their
approximate cost would be if you were to
buy them on eBay and telling you what I
paid for them I don't think would be all
that helpful because you know like I say
I've had a lot of this junk in my shop
for a long time and some of it was you
know found or donated or repaired or
whatever so I'll try to give you the
eBay cost for most of these so let's
start at the top the tungsten filament
is a relatively simple thing it's just a
piece of wire in fact my original plan
was to use tungsten wire and just bend
it into a filament shape and call it a
day
the problem with that is that you have
to
yo filaments burn out and you have to
make new filaments and if the size is a
little bit off it might take a long time
to realign so I opted and then the other
problem is you need some kind of an
insulator so you either custom machine
your own ceramic or whatever it gets
pretty complicated so what I opted to do
especially because I found these is just
by the filaments premade off eBay so
these are actual electron microscope
filaments and as you can see they come
in a pack because they do burn out
pretty often you know 40 hours of use or
something is not unreasonable and it
comes with this nice ceramic insulator
so I was able to design an electron gun
that would just accept this right away
and be really easy these are pretty
cheap I think I spent about $30 or
something for this whole box of
filaments so we'll start there
and like you say you there's absolutely
nothing wrong with with making your own
filaments you can just bend that stuff
into the shape and be all set let's put
down 30 bucks for the filament now you
need a power supply for the filament and
this you'll probably have to build
there's really no ready-made power
supply that's going to do what we want
what we need is DC it can't be AC I
originally built an AC power supply for
it and it didn't work so I had to
rectify it I don't know why we'll talk
about that later you basically have a
six volt like you know 115 to six volt
transformer so a low-voltage X former
and then you need some way of adjusting
the voltage I used to variac can be a
pretty small very accidents we're not
talking huge current and then you also
need an isolation transformer since
Variax do not isolate and the other side
of this filament is going to be
connected to high voltage so you can't
you can't go straight through you need
an isolation transformer I think the
parts cost was probably under a hundred
dollars we'll just put down a hundred to
be to be sure the next guy is the sort
of the main power supply for the
of the electrons and this is like a 0 to
10 kV would be a good supply DC it has
to be very tightly regulated it can't be
an unregulated power supply so like a
flyback with a capacitor on it's not
going to do it it actually needs to be
regulated again my power supply is more
or less found for for very low cost at a
flea market but there are good power
supplies on ebay in this range and they
aren't so bad so we'll put down 100
bucks for that and I'll talk about what
I used off eBay too and in just a minute
the condenser lens it's something you're
going to machine from parts and we're
not talking about machining or parts yet
this is just the block components so
moving on we have the scan plates the
deflection plates and you'll need a
raster generator to drive those this is
also something you'll probably have to
build I actually would have been really
happy to buy this and in the comments
we've been talking about doing a digital
version of this thing and instead of
using like an analog oscilloscope with
all this you can do it all digitally
with an FPGA or something and that is
actually a good idea I wouldn't mind
doing that but anyway for the raster
generator you know you need like a 400
volt supply inside here and some
transistors and stuff and I'll talk
about more that in the sources later why
don't we put down another 100 bucks for
the parts in there the focus power
supply this is also like 0 to 10 kV
we're going to put down 70 for that one
on eBay if you search for Spellman power
supply there's a negative 6 kV 2 + 10 kV
supply that no one seems to want to buy
because the part number is like a custom
part number they're available now or at
least last I checked there's at least
one or two still on eBay but luckily the
pin out and all the voltages are written
right on the side of the power supply
case so it's actually a little bit
cheaper than most other high voltage
regulated power supplies on eBay ok then
we have the photomultiplier itself this
is the one that I used it is a
hammamet's ooh
r60 94609 for I don't think there's any
more of these on eBay but there might be
I only paid about $35 for this which is
a little bit lower than the average but
not much you can go on eBay and find
photomultiplier tubes for 450 bucks so
we'll put down 50 for that and then you
need a power supply to drive it this I
did buy off eBay very recently and I
spent about a hundred dollars for that
it's a five two hundred volts to two
thousand volts or something like that
it's a rack-mounted power supply then
you need a power supply for the Faraday
cage on the secondary detector this can
be zero to a thousand volts also tightly
regulated DC I think I probably spent
about fifty on that for off of ebay then
you need a phosphor the accelerating
power supply this can be it doesn't have
to be adjustable this one can just be
ten kilovolts again I think I use one of
these Spellman's too so we'll put down
70 bucks for that then you need the
actual phosphor this is another part
that you really can't cheat on so I went
to an electron microscope supply house
and just bought the little phosphor disk
and I would show it to you but sadly I
ruined the thing in a very stupid way
but but it actually still works
surprisingly so those images that I
showed in my last video were made with
the broken phosphor disc anyway that was
I think that's about $90 the phosphor
now at the bottom of the microscope and
I haven't talked about this yet what
most microscopes have like a mechanical
stage that moves the specimen around so
I bought a couple of those off eBay
not really I haven't even hooked them up
yet you know you can move the scan
pattern around electronically but that
only goes so far so it's really nice er
to have a mechanical means as well so
put down 150 for the pair of stages you
don't you could build them yourself to
this there's nothing wrong with that
okay so now below this dotted line here
this is
like the vacuum system this is just the
electron microscope section so we're
talking vacuum down here you need some
kind of a chamber I honestly forget how
much I spent for that glass bell jar but
I wouldn't recommend glass anyway really
a metal column would be a much better
choice so I'm going to leave that one
blank because they who knows how much
that is but you do need a high vacuum
gauge and I used a penning gage um and I
spent about 175 on that I think a while
back I've had it for a long time and
then you need a high vacuum pump in my
case I used a diffusion pump which is
good because they're cheap and very
robust it's hard to kill those things
diffusion pump you know the one that I
used was a three-inch diffusion pump
which is you know pretty good size for
that chamber but it could be a little
bit bigger don't bother with the
two-inch diffusion pumps go for a for at
least three or four these are available
on eBay and like you say it just kind of
depends on the the atmosphere sometimes
you might get one for a hundred bucks
just other times not let's put down
let's put down 200 why not and then you
need a mechanical pump these are
actually much easier to find you can get
a mechanical pump that's meant for air
conditioning service that's that's great
so those are those are good pumps for
that so put down 200 get yourself a
brand new one for that and like I say
this this you know cost breakdown really
doesn't cover any of the like the parts
parts like the Teflon for these
insulators and the metal and the rods
and adjustment stuff these are just sort
of the big-ticket items that you really
can't get around and I got my you know
if you really want to shock just look
into the cost of some of these things
this is really cheap high vacuum grease
but the really high quality stuff is
like fifty dollars for like a one ounce
tube so I mean you know there's a lot of
crazy costs involved you don't have to
go overboard
so I guess I should add all these up for
you I guess I'll do that in
post-production because I want to do it
right now and in the next video I'll get
into more detail with each one of these
things and again bring up cost but this
is just to give you a really basic idea
and I'll also compile a list of sources
so that you can see where I got my
information to build this thing all
right well feel free to post any
questions you have thanks for watching

and I will see you next timeTop Paid Keyword :  earn cash online, google make money from home, earn money online without investment by clicking ads, free earn money website, online money making jobs, earn money online without investment by typing, online work for money, best online earning sites, make money online with google, online earning websites, money making websites, online earning websites for students, invest online and earn money, best online money making, online money income, view ads and earn money without investment, earn money online by clicking, online money income site, money earning sites, online earning sites, best website to earn money,

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