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Wednesday, January 8, 2020

Freeze-drying Jello gelatin with an improved cold trap--- make money online

Freeze-drying Jello gelatin with an improved cold trap--- make money online

okay so here we have freeze-dried jell-o
gelatin so this came out pretty similar
to the astronaut ice cream but of course
this is fat-free
it's just gelatin and water and sugar so

the structure is a little a little more
rigid and breakable even than the
astronaut ice cream I think there's
still some fat left in the ice cream
that makes it kind of a little bit
softer when even in its freeze-dried
form so let's try one of these out not
bad it's pretty good candy I mean it's
it has a lot of sugar and artificial
flavoring in there so that's it's done
kind of melts in your mouth
very light yeah thumbs up so in my
previous video where I made the
astronaut ice cream I had a problem with
the cold trap that I used originally I
had this copper pipe connected to the
vacuum hoses and I submerged the copper
pipe into an isopropanol bath in this
vacuum flask and then filled it up with
dry ice so the idea is that as the water
vapor travels through the copper pipe it
will condense or solidify inside here
and prevent it from going through the
vacuum pump the problem was that so much
water came out of the ice cream that the
copper pipe completely plugged up so
this cold trap isn't big enough to hold
all the water that we're pulling out of
the food so what I wanted to do is build
a much larger cold trap that could hold
more water so I went to Target and
bought a set of three of these very
cheap aluminum pots or kind of saucepans
I guess at that this at the store and
three of these came together and they
were all kind of nested together and I
thought oh that's good because that's
that's pretty much the shape that I want
this cold trap is built with the inlet
and outlet here and then the idea is
that you put another container and the
inside like this and put your cold
substance inside here and then pump out
the air that's in the larger one so it's
kind of like we're building a thermos
here actually is how it works because
they'll be vacuum between the outside
and the inside and then this will be
where the cold where the cold stuff goes
so originally I was just going to use
two of the three that I buy because
they're already nested but then I
thought well you know actually this
internal one shouldn't be aluminum
because it's going to conduct heat too
well so I looked around the shop and
found an even better solution and so I
used this stainless steel pan instead
this is a very thin walled stainless
steel pan and stainless steel is
actually a very poor conductor of heat
which is what we want in this case so
this fits down in here like this and
when the vacuum is pulled this whole
thing seals down and when I put
isopropanol and dry ice in here the
temperature at the at the rim is cold
but it's not it wouldn't be as cold as
if I had used aluminum especially this
relatively thick aluminum pan here this
would conduct too much heat out to the
rim whereas the stainless steel actually
helps retain the the coldness of the of
the isopropanol bath where it's needed
so unfortunately I don't have any video
of me making this because the camera ran
out of batteries and I didn't want to
wait so what I did is I just machined
some aluminum pipe fittings here these
these were just turned out of a solid
piece of aluminum and I welded them on
to the pilot of the pan after drilling a
hole in it and then I welded on these
mounting ears to help screw this piece
of acrylic down so there's a rubber
gasket between the acrylic and the
aluminum pan and it's just held down
these screws when the thing is under
vacuum will be a lot of force pushing
this down anyway so the screws are just
to kind of keep everything in place so
to test it out I made some jello in one
of these Erlenmeyer flasks and I scaled
it from the package a package makes four
and a half cups
prepared so I've measured it out and I
think that comes out to about 18 grams
of jello for 100 milliliters total of
water so 50 mils of boiling water and 50
mils of cold water so I prepared it as
the package recommends and then put the
flask into the refrigerator for a while
and the next day or later that evening I
took it out and put it into the water
cooler with dry ice and isopropanol in
it just to freeze it as quickly as
possible so within a half an hour it was
solid frozen and I hooked it up to the
vacuum system and then added dry ice and
isopropanol to the cold trap and let it
freeze dry for about 18 hours in this
case the flask or the jello is in such
good thermal contact with the flask wall
I didn't have to heat it like I did with
the ice cream so in this case the the
gelatin was was so well connected with
the glass of the flask I could actually
just leave it out on the table even with
a little insulation to keep it from
getting too warm with the ice cream it
was not connected well with the flask
and so it would keep itself cold just
from being in a vacuum in the flask so
for the first probably eight hours of
the freeze drying I just left it with
inside a piece of styrofoam just to keep
the flask from warming up too quickly
and then later I eventually resorted to
putting it under a lamp to get the last
bit of water out when I took the cold
trap apart to see how much water had
accumulated in there I was surprised to
see that even this design of cold trap
that doesn't seem to be enough to hold a
significant amount of water as you can
see the ice was formed in a shape that
was almost ready to plug the thing up
again I really couldn't believe it I I
knew there would be a concentration of
ice on that side of the cold trap
because that's where the inlet is but I
didn't think it was going to be quite so
pronounced so I think in the future
I'll have to design this with like a a
dent or a an indentation or some kind of
a specially shaped internal structure
that can accommodate a lot more water
it's also not very efficient I went
through about seven pounds of dry ice in
total just because of the heat leakage
through the plastic it causes the
isopropanol to boil i rep causes the dry
ice to sublimate slowly and it takes
that much okay I think I'm going to try
some fruit next since I got some
interesting suggestions about freeze
drying fruit so I'll give that a shot
and of course the vacuum frying and
pressure frying and see what other kind
of weird foodstuff we can do okay see

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