Supercritical CO2 caffeine extraction (negative result -- more work needed)--- make money online

hey everyone I know no one likes to see

negative results but I think it's always

important to publish these things so

that you know what not to do what I'm I

attempted was to extract caffeine from

green coffee beans so I got some green

coffee beans and I got this tank here

which is made for paintball guns this is

made to hold nitrogen compressed

nitrogen at 3,000 psi so it's actually

built it with a heavier construction

than the co2 tanks so I originally

thought I was going to cut this thing

with a bandsaw and then weld some

flanges to it so that I could open the

tank up and use it as a high-pressure

vessel but the the tank is quite thick

and I was worried that welding it would

affect the strength of the metal and

also welding something so thick would be

tricky with my welder I would have to

preheat this but I may still try it so

that that'll be a topic for another

video so anyway the first order of

business is cleaning this thing out i

unscrewed the valve came with a pressure

gauge and a valve on the top unscrewed

this and looked in there and found all

kinds of crap so I figured one of the

best ways to clean this would be to put

some steel shot in there with some

cleaning solution and then mounted on

the lathe and have it spin around so

that the shot would hit the wall of the

chamber and kind of clean it off so that

works pretty well so next I wanted to do

a dry run so I packed this thing up with

some dry ice and didn't really measure

too much I just wanted to make sure that

there was some dry ice in there to make

a supercritical fluid and that way I

could you know swish it around in there

and then dump and then release the

pressure slowly and pour out the the

solvent to sort of clean the chamber so

I did that and put it in the oven and

raised the temperature made sure it went

supercritical took it out brought it

back down and poured out the the solvent

I had some water and ethanol in there

just as a basic solvent and that helped

that cleaned out some more gunk out of

the out of the chamber so then I was

ready and I got some green coffee beans

and put those in the chamber

and then again packed in some more dry

ice ground up dry ice and then I also

added some ethanol and water vodka in

this case as that has a co solvent so I

read online that oftentimes ethanol and

water is used in conjunction with

supercritical co2 to to extract caffeine

and I should have been measuring all

this but I really wasn't just put it all

together and then put it in the oven for

a total of about six hours so it was

about eighty degrees C for six hours and

opened it up and very slowly shook out

all of the beans they actually changed

quite a bit the beans that came out of

the chamber were almost like hard rubber

like they were white discolored from the

original green of the green coffee beans

and there was no solvent left even

though I poured in some some water and

ethanol when I took the chamber out of

the oven

only rubberized the beans came out I

actually didn't get any liquid out

whatsoever which was surprising so I got

the beans into a funnel with a filter

and then I was thinking well the

caffeine probably went into the solution

in the supercritical co2 and when I

released the pressure all that caffeine

probably came out of solution and stuck

to the outsides of the beans so now all

I have to do is wash it off right so I

had the beans in that funnel and poured

just some water over them and let it

drain out so then I had a solution of

what I thought was dirty caffeinated

water so I poured that into a pan and

set it up on the stove thinking that I

would evaporate most of it away through

boiling and then the last bit could be

evaporated just by him straight

evaporation and then I could you know

scrape off the crystals well

unfortunately there were no crystals to

scrape off there was absolutely no

detectable caffeine I I forget what the

solubility is but it's it's some number

of grams per per liter

anyway I'll look it up but I could tell

that there was absolutely no

precipitation going on whatsoever so

there was basically no caffeine in that

panel

water so anyway I I think I will follow

up by trying something else maybe I

actually will convert this chamber to be

more of a a chamber and then I can put

more solvent in the and the bottom I

think a lot of commercial co2 or

supercritical co2 decaffeination works

by having like a bunch of water and

ethanol at the bottom of the chamber and

the beans are suspended above and like a

mesh net or something and then the

supercritical co2 passes through the

beans through the water and transfers

the caffeine into the water so maybe

I'll try something like that anyway I

just thought I would share this to show

you what what doesn't work and for my

next trick I might actually try aerogel

someone sent me some information about

aerogels and so if I cut this chamber up

so that I can actually access the hole

the hole inside I think that might be

something pretty fun to try - alright

see you next time bye best online income, earn money online data entry, easy ways to make money online, best online earning websites, top websites to earn money, online typing jobs for students to earn money, earn skrill money online, earn skrill money, best way to earn money from home, make instant money online absolutely free, trusted online money making sites, online income site, best online earning, money online, earn money from home, earn dollars online, earn money online, earn money online 2019, earn money online by typing pages, earn money online daily, online work at home and earn money, online earning, earn money online free, online money earning sites, earn real money online, e commerce ideas to make money, easiest way to earn money online,